A Convenient Alternative Route for the Synthesis of Bis(2,5-dimethylpyrrolo[3,4-d])tetrathiafulvalene

Marta Vico Solano; Mogens B. Nielsen; Jan Oskar Jeppesen

doi:10.1002/jhet.2046

A Convenient Alternative Route for the Synthesis of Bis(2,5-dimethylpyrrolo[3,4-d])tetrathiafulvalene

Marta Vico Solano
, Mogens B. Nielsen
, Jan Oskar Jeppesen

Institut for Fysik, Kemi og Farmaci

Københavns Universitet

Publikation: Bidrag til tidsskrift › Tidsskriftartikel › Forskning › peer review

Abstract

An alternative and efficient protocol for the synthesis of methylated pyrrolo-tetrathiafulvalenes have been developed. The key intermediate in this new synthetic protocol is 4,6-dimethyl-N-tosyl-(1,3)-dithiolo[4,5-c]pyrrole-2-one, which can be obtained in high yield in a three-step synthetic procedure from 5-dimethyl-3,4-dithiocyanopyrrole.

Originalsprog	Engelsk
Tidsskrift	Journal of Heterocyclic Chemistry
Vol/bind	53
Udgave nummer	3
Sider (fra-til)	915–918
ISSN	0022-152X
DOI	https://doi.org/10.1002/jhet.2046
Status	Udgivet - 2016

Dokumenter og links

10.1002/jhet.2046

SDU link

Tjek adgangen til materialet i Syddansk Universitetsbiblioteks søgemaskine

Citationsformater

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title = "A Convenient Alternative Route for the Synthesis of Bis(2,5-dimethylpyrrolo[3,4-d])tetrathiafulvalene",

abstract = "An alternative and efficient protocol for the synthesis of methylated pyrrolo-tetrathiafulvalenes have been developed. The key intermediate in this new synthetic protocol is 4,6-dimethyl-N-tosyl-(1,3)-dithiolo[4,5-c]pyrrole-2-one, which can be obtained in high yield in a three-step synthetic procedure from 5-dimethyl-3,4-dithiocyanopyrrole.",

author = "Solano, \{Marta Vico\} and Nielsen, \{Mogens B.\} and Jeppesen, \{Jan Oskar\}",

year = "2016",

doi = "10.1002/jhet.2046",

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journal = "Journal of Heterocyclic Chemistry",

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T1 - A Convenient Alternative Route for the Synthesis of Bis(2,5-dimethylpyrrolo[3,4-d])tetrathiafulvalene

AU - Solano, Marta Vico

AU - Nielsen, Mogens B.

AU - Jeppesen, Jan Oskar

PY - 2016

Y1 - 2016

N2 - An alternative and efficient protocol for the synthesis of methylated pyrrolo-tetrathiafulvalenes have been developed. The key intermediate in this new synthetic protocol is 4,6-dimethyl-N-tosyl-(1,3)-dithiolo[4,5-c]pyrrole-2-one, which can be obtained in high yield in a three-step synthetic procedure from 5-dimethyl-3,4-dithiocyanopyrrole.

AB - An alternative and efficient protocol for the synthesis of methylated pyrrolo-tetrathiafulvalenes have been developed. The key intermediate in this new synthetic protocol is 4,6-dimethyl-N-tosyl-(1,3)-dithiolo[4,5-c]pyrrole-2-one, which can be obtained in high yield in a three-step synthetic procedure from 5-dimethyl-3,4-dithiocyanopyrrole.

U2 - 10.1002/jhet.2046

DO - 10.1002/jhet.2046

M3 - Journal article

SN - 0022-152X

VL - 53

SP - 915

EP - 918

JO - Journal of Heterocyclic Chemistry

JF - Journal of Heterocyclic Chemistry

IS - 3

ER -

A Convenient Alternative Route for the Synthesis of Bis(2,5-dimethylpyrrolo[3,4-d])tetrathiafulvalene

Abstract

Dokumenter og links

SDU link

Fingeraftryk

Citationsformater